Reaction #43712

ord-92624d1e680540a998df40eb5b5b9df9

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Procedure

Using 1.0 g (6.31 mmol) of 2-fluoro-3-chlorobenzaldehyde, 0.38 g (9.46 mmol) of sodium hydride (60% pure) and 0.74 g (6.94 mmol) of methyl mercaptoacetate, 1.04 g (72.3% of theory) of the title compound are obtained.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07732477B2uspto-grants-2010_06