Reaction #432442

ord-b586495e75b64103b8ef0e456075ea8c

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Workup

  1. 1
    OtherThe same isocyanuration reaction as in Production Example 1

Procedure

The same isocyanuration reaction as in Production Example 1 was carried out except that 3,290 g of hexamethylene diisocyanate and 210 g of "Takenate 500" (xylylene diisocyanate produced by Takeda Chemical Industry Co., Ltd.) were used instead of 3,500 g of hexamethylene diisocyanate, and the amount of the isocyanuration catalyst used in production Example 1 was changed to 4.7 g. There was obtained 4,219 g of the reaction mixture containing the deactivated catalyst.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US05055514uspto-grants-1991_10