Reaction #417905
ord-539659cc286943089e7eb0f073eca70f
Reaction equation
Desmorapid
n-butyl isocyanate
isocyanate
→
Ethyl butylcarbamate
Reagents
None
Solvents
Conditions
Temperature
60°CELSIUS
Detailed conditions
See reaction.notes.procedure_details.
Workup
- 1TemperatureThereafter, cooling
- 2Otherthe product was obtained as a clear liquid
Procedure
In a 250 ml round-bottomed flask, 0.02 g of Desmorapid Z, 34.1 g of n-butyl isocyanate were initially introduced and heated to 60° C. Thereafter, 15.9 g of ethanol were added dropwise and the mixture was further kept at 60° C. until the isocyanate content had fallen below 0.1%. Thereafter, cooling was effected and the product was obtained as a clear liquid.