Reaction #411558

ord-f2b990ef9a7f446f900cdb6bd478ee18

Reaction equation

CCOC=C(C#N)C#N
ethoxymethylenemalononitrile
NNc1c(Cl)cc(Cl)cc1Cl
2,4,6-trichlorophenylhydrazine
N#Cc1cnn(-c2c(Cl)cc(Cl)cc2Cl)c1N
title compound
N#Cc1cnn(-c2c(Cl)cc(Cl)cc2Cl)c1N
5-amino-1-(2,4,6-trichlorophenyl)-1H-pyrazole-4-carbonitrile

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Procedure

The title compound was prepared as an orange solid, m.p. 208.5-209.5° C. by the procedure of Preparation A starting with ethoxymethylenemalononitrile and 2,4,6-trichlorophenylhydrazine.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06218397B1uspto-grants-2001_04