Reaction #40307

ord-1b11742f473c477887fee3c6574fe70c

Reaction equation

CCOC(=O)CC1CCCCC1=O
ethyl(2-oxo-cyclohexyl)-acetate
CC(C)(C)C1CCCC(Cl)C1=O
2-tert-butyl-6-chloro-cyclohexanone
→
CCOC(=O)CC1CCCC(Cl)C1=O
title compound
CCOC(=O)CC1CCCC(Cl)C1=O
Ethyl(3-chloro-2-oxo-cyclohexyl)-acetate

Reactants

CCOC(=O)CC1CCCCC1=O
ethyl(2-oxo-cyclohexyl)-acetate
CC(C)(C)C1CCCC(Cl)C1=O
2-tert-butyl-6-chloro-cyclohexanone
—
crude product

Reagents

None

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Procedure

The chlorination of ethyl(2-oxo-cyclohexyl)-acetate takes place in a manner similar to that described above for the preparation of 2-tert-butyl-6-chloro-cyclohexanone. The title compound is reacted as a crude product without further characterization.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07727979B2uspto-grants-2010_06