Reaction #3833

Reaction equation

2,2'-dithiobisbenzoyl chloride

pyrrolidine

triethylamine

→

title compound

Yield 60.6%

{2-[2-(pyrrolidine-1-carbonyl)-phenydisulfanyl]-phenyl}-pyrrolidin-1-yl-methanone

Yield 60.6%

Solvents

dichloromethane

dichloromethane

Conditions

Workup

1. 1
   OtherThis compound was prepared

Procedure

This compound was prepared according to the general method of Example 112 using 2,2'-dithiobisbenzoyl chloride (1.0 g, 3.0 mmol) in 15 mL of dichloromethane and pyrrolidine (0.63 mL, 7.5 mmol) and triethylamine (1.2 mL, 9 mmol) in 20 mL of dichloromethane, to give 0.75 g of the title compound as a foam, mp 62°-63° C.;

Source