Reaction #336847

ord-44e11de5cdfd4e08be52342d10bd0da0

Reaction equation

N[C@@H](Cc1ccc(O)c(O)c1)C(=O)O
3,4-dihydroxyphenylalanine
N[C@@H](Cc1ccc(O)c(O)c1)C(=O)O
L-dopa
O=C1C=C2CC(C(=O)O)NC2=CC1=O
dopachrome

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Procedure

To a 96-well plate, 40 μl of mushroom-derived tyrosinase (125 unit/ml; dissolved in a 67 mmol/l phosphate buffer solution; Sigma), 120 μl of 3,4-dihydroxyphenylalanine that serves as a substrate (L-dopa; 5 mmol/l; dissolved in a 67 mmol/l phosphate buffer solution; Sigma), and 40 μl of an inhibitor solution were added. The plate was allowed to stand for 37° C. for 30 minutes. Then, the amount of dopachrome produced was determined by absorbance at 490 nm. Tyrosinase inhibitory activity was expressed as an inhibitory rate obtained by the following equation: Inhibitory Rate (%)=[(A−B)−(C−D)]/(A−B)×100

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07863248B2uspto-grants-2011_01