Reaction #324358

Reaction equation

aniline

propane sultone

→

3-phenylammonio-1-propanesulfonate

Yield 95.0%

Solvents

acetonitrile

Conditions

Workup

1. 1
   Filtrationthe solid of 3-phenylammonio-1-propanesulfonate was filtered
2. 2
   Otherair-dried

Procedure

A mixture of aniline (7 mmol) and propane sultone (10 mmol) was heated in 10 mL of acetonitrile at 12.0-130° C. for 9 h in a pressure tube under argon atmosphere. The product was allowed to cool to room temperature and the solid of 3-phenylammonio-1-propanesulfonate was filtered and air-dried. Yield: 95%.

Source