Reaction #312581

ord-8361219c12a249c08926f238d10d0e29

Reaction equation

O=C(Cl)CCCCCl
5-chlorovaleryl chloride
CCC1(O)C2CC3CC(C2)CC1C3
2-ethyl-2-adamantanol
O=C(Cl)CCl
chloroacetyl chloride
CCC1(O)CCCCC1
1-ethyl-1-cyclohexanol
C=C(C)C(=O)OCCCCC(=O)OC1(CC)CCCCC1
4-(1-ethyl-1-cyclohexyloxycarbonyl)butyl methacrylate

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Workup

  1. 1
    Otherwas obtained

Procedure

Synthetic experiment was conducted in the same manner as in Monomer Synthesis Example 1 except that 2-ethyl-2-adamantanol and chloroacetyl chloride were changed to 1-ethyl-1-cyclohexanol and 5-chlorovaleryl chloride respectively, and the above described methacrylic derivative was obtained.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07556908B2uspto-grants-2009_07