Reaction #312578

ord-af992dc82f6e48159b9f100e48e953ed

Reaction equation

O=C(Cl)CCCCl
4-chlorobutyryl chloride
CCC1(O)C2CC3CC(C2)CC1C3
2-ethyl-2-adamantanol
O=C(Cl)CCl
chloroacetyl chloride
CCC1(O)CCCC1
1-ethyl-1-cyclopentanol
C=C(C)C(=O)OCCCC(=O)OC1(CC)CCCC1
3-(1-ethyl-1-cyclopentyloxycarbonyl)propyl methacrylate

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Workup

  1. 1
    Otherwas obtained

Procedure

Synthetic experiment was conducted in the same manner as in Monomer Synthesis Example 1 except that 2-ethyl-2-adamantanol and chloroacetyl chloride were changed to 1-ethyl-1-cyclopentanol and 4-chlorobutyryl chloride respectively, and the above described methacrylic derivative was obtained.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07556908B2uspto-grants-2009_07