Reaction #2537

ord-29a2732da3a948f4aae1ec2e95eeccf2

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Procedure

Using 4-fluoroaniline (1.1 ml, 10.9 mmol) and 3-nitrobenzoic acid (1.76 g, 10.0 mmol), the procedure of Reference Example 16 was repeated to obtain 1.98 g (76.0%) of the title compound in the form of light yellow needle crystals.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US05728835uspto-grants-1998_03