Reaction #2536

ord-f1ead6dddb964cfda207e6e2ba7f29ba

Reagents

None

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Procedure

Using p-toluidine (1.19 g, 11.0 mmol) and 3-nitrobenzoic acid (1.76 g, 10.0 mmol), the procedure of Reference Example 16 was repeated to obtain 2.27 g (88.3%) of the title compound in the form of colorless needle crystals.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US05728835uspto-grants-1998_03