Reaction #2534

ord-6dae5ade71d64ef5bed47b84c6e2b2bc

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Procedure

Using 4-fluoroaniline (1.0 ml, 9.93 mmol) and 4-nitrobenzoic acid (1.58 g, 9.36 mmol), the procedure of Reference Example 16 was repeated to obtain 1.60 g (65.8%) of the title compound in the form of light yellow needle crystals.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US05728835uspto-grants-1998_03