Reaction #2492967

ord-28e8315f77b64fecafa51d64c0b249b4

Reaction equation

NS(=O)(=O)Oc1ccccc1
sulfamic acid phenyl ester
CCC1(O)CC1
1-ethylcyclopropanol
CCC1(OS(N)(=O)=O)CC1
sulfamic acid 1-ethyl-cyclopropyl ester

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Workup

  1. 1
    OtherSulfamic acid 1-ethyl-cyclopropyl ester was synthesized

Procedure

Sulfamic acid 1-ethyl-cyclopropyl ester was synthesized according to the method presented in the synthesis of sulfamic acid phenyl ester in Example 1 with the exception of utilizing 1-ethylcyclopropanol (synthesized by methods reported in Synthesis 1991, 234) to obtain sulfamic acid 1-ethyl-cyclopropyl ester.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08809267B2uspto-grants-2014_08