Reaction #2383763

ord-dd422b610fdf444eaffdb5e45e3e760d

Reagents

None

Solvents

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Workup

  1. 1
    OtherWater and methanol were then evaporated

Procedure

96 g (1.0 mol) of 3,4-dimethylpyrazole in 50 ml of methanol were dissolved in 100 g (1.0 mol) of formalin solution (30%) at room temperature. Water and methanol were then evaporated. The title compound remained as a white solid (yield 95%).

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06488734B1uspto-grants-2002_12