Reaction #2354235

ord-6070c006cad640c9b36bf0edf7932479

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Procedure

Using the method of Preparation 155 using (4-mercaptophenyl)methanol (10.0 g, 71.3 mmol) and 5-bromopicolinonitrile (13.0 g, 71.3 mmol) affords the title compound (4.90 g, 28%).): 243 (M+H, 100%).

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07858646B2uspto-grants-2010_12