Reaction #2329038

ord-2efc181edf924ec9a8b065fcbc3c2897

Reaction equation

CCOc1ccc(CCl)cc1
4-ethoxybenzyl chloride
O=S(Cl)Cl
thionyl chloride
CCCCCCCCOc1ccc(CO)cc1
4-octyloxybenzyl alcohol
→
CCCCCCCCOc1ccc(CCl)cc1
4-Octyloxybenzyl Chloride

Reactants

CCOc1ccc(CCl)cc1
4-ethoxybenzyl chloride
O=S(Cl)Cl
thionyl chloride
CCCCCCCCOc1ccc(CO)cc1
4-octyloxybenzyl alcohol

Reagents

None

Solvents

ClCCl
CH2Cl2

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Workup

  1. 1
    OtherThis compound was synthesized

Procedure

This compound was synthesized following the same general procedure as that for the preparation of 4-ethoxybenzyl chloride; thionyl chloride (6.36 g, 53.4 mmol), 4-octyloxybenzyl alcohol (12.4 g, 52.5 mmol), CH2Cl2 (150 mL).

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07671033B2uspto-grants-2010_03