Reaction #2329037

ord-73663425d1c5459c94f29258d3cba0d7

Reaction equation

CCOc1ccc(CCl)cc1
4-ethoxybenzyl chloride
O=S(Cl)Cl
thionyl chloride
CCCCCCOc1ccc(CO)cc1
4-hexyloxybenzyl alcohol
→
CCCCCCOc1ccc(CCl)cc1
4-Hexyloxybenzyl Chloride

Reactants

CCOc1ccc(CCl)cc1
4-ethoxybenzyl chloride
O=S(Cl)Cl
thionyl chloride
CCCCCCOc1ccc(CO)cc1
4-hexyloxybenzyl alcohol

Reagents

None

Solvents

ClCCl
CH2Cl2

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Workup

  1. 1
    OtherThis molecule was synthesized

Procedure

This molecule was synthesized following the same general procedure as that for the preparation of 4-ethoxybenzyl chloride; thionyl chloride (7.17 g, 60.3 mmol), 4-hexyloxybenzyl alcohol (11.3 g, 54.3 mmol), CH2Cl2 (150 mL).

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07671033B2uspto-grants-2010_03