Reaction #2329036

ord-9bd1e1d60ac142fbbaacce3d10513730

Reaction equation

CCOc1ccc(CCl)cc1
4-ethoxybenzyl chloride
O=S(Cl)Cl
thionyl chloride
CCCCOc1ccc(CO)cc1
4-butoxybenzyl alcohol
→
CCCCOc1ccc(CCl)cc1
4-Butoxybenzyl Chloride

Reactants

CCOc1ccc(CCl)cc1
4-ethoxybenzyl chloride
O=S(Cl)Cl
thionyl chloride
CCCCOc1ccc(CO)cc1
4-butoxybenzyl alcohol

Reagents

None

Solvents

ClCCl
CH2Cl2

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Workup

  1. 1
    OtherWas synthesized

Procedure

Was synthesized following the same general procedure as that for the preparation of 4-ethoxybenzyl chloride; thionyl chloride (7.42 g, 69.2 mmol), 4-butoxybenzyl alcohol (9.45 g, 52.4 mmol), CH2Cl2 (145 mL).

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07671033B2uspto-grants-2010_03