Reaction #2320109

ord-3c38614e047e4282b46fca1c66441759

Reaction equation

FC(F)(F)c1cc(Cl)cc(N2CCNCC2)c1
1-(3-Chloro-5-trifluoromethyl-phenyl)-piperazine
C=CCBr
allylbromide
C=CCN1CCN(c2cc(Cl)cc(C(F)(F)F)c2)CC1
1-Allyl-4-(3-Chloro-5-trifluoromethyl-phenyl)-piperazine

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Workup

  1. 1
    Otherthe title compound was recovered by the procedure

Procedure

Beginning with 1-(3-Chloro-5-trifluoromethyl-phenyl)-piperazine and allylbromide, the title compound was recovered by the procedure described in Example 2. MS m/z (rel. intensity, 70 eV)) 305 (M+, 7), 96 (57), 69 (bp), 68 (48), 56 (69).

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: USRE041315E1uspto-grants-2010_05