Reaction #2320098

ord-5332abc6f8cb466188789e97994fab6d

Reaction equation

COc1ccc(N2CCNCC2)cc1S(C)(=O)=O
1-(3-Methanesulfonyl-4-methoxy-phenyl)-piperazine
CCI
Et-I
→
CCN1CCN(c2ccc(OC)c(S(C)(=O)=O)c2)CC1
1-Ethyl-4-(3-Methanesulfonyl-4-methoxy-phenyl)-piperazine

Reactants

COc1ccc(N2CCNCC2)cc1S(C)(=O)=O
1-(3-Methanesulfonyl-4-methoxy-phenyl)-piperazine
CCI
Et-I

Reagents

None

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Workup

  1. 1
    Otherthe title compound was recovered by the procedure

Procedure

Beginning with 1-(3-Methanesulfonyl-4-methoxy-phenyl)-piperazine and Et-I, the title compound was recovered by the procedure described in Example 2: MS m/z (rel. intensity, 70 eV)) 298 (M+, 81), 283 (45), 84 (36), 57 (bp), 56 (41).

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: USRE041315E1uspto-grants-2010_05