Reaction #2320097

ord-cd2181d10b064f0e94aa888dc235ca27

Reaction equation

COc1ccc(N2CCNCC2)cc1S(C)(=O)=O
1-(3-Methanesulfonyl-4-methoxy-phenyl)-piperazine
CCCCBr
n-Bu-Br
→
CCCCN1CCN(c2ccc(OC)c(S(C)(=O)=O)c2)CC1
1-Butyl-4-(3-Methanesulfonyl-4-methoxy-phenyl)-piperazine

Reactants

COc1ccc(N2CCNCC2)cc1S(C)(=O)=O
1-(3-Methanesulfonyl-4-methoxy-phenyl)-piperazine
CCCCBr
n-Bu-Br

Reagents

None

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Workup

  1. 1
    Otherthe title compound was recovered by the procedure

Procedure

Beginning with 1-(3-Methanesulfonyl-4-methoxy-phenyl)-piperazine and n-Bu-Br, the title compound was recovered by the procedure described in Example 2; MS m/z (rel. intensity, 70 eV)) 326 (M+, 32), 284 (16), 283 (bp), 70 (58), 56 (23).

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: USRE041315E1uspto-grants-2010_05