Reaction #2320083

ord-b866565e36fc493a9fe28e1d0068035e

Reaction equation

FC(F)(F)c1ccc(Cl)c(N2CCNCC2)c1
1-(2-Chloro-5-trifluoromethyl-phenyl)-piperazine
CCCI
1-iodopropane
→
CCCN1CCN(c2cc(C(F)(F)F)ccc2Cl)CC1
1-(2-Chloro-5-trifluoromethyl-phenyl)-4-propyl-piperazine

Reactants

FC(F)(F)c1ccc(Cl)c(N2CCNCC2)c1
1-(2-Chloro-5-trifluoromethyl-phenyl)-piperazine
CCCI
1-iodopropane

Reagents

None

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Workup

  1. 1
    Otherthe title compound was recovered by the procedure

Procedure

Beginning with 1-(2-Chloro-5-trifluoromethyl-phenyl)-piperazine and 1-iodopropane, the title compound was recovered by the procedure described in Example 2. m.p. 234° C. (HCl), MS m/z (rel. intensity, 70 eV) 306 (M+, 20), 279 (34), 277 (bp), 70 (99), 56 (48).

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: USRE041315E1uspto-grants-2010_05