Reaction #2320077

ord-a7d4e2464276428ba533abc94137ea18

Reaction equation

FC(F)(F)c1cc(Cl)cc(N2CCNCC2)c1
1-(3-Chloro-5-trifluoromethyl-phenyl)-piperazine
CCI
iodoethane
CCN1CCN(c2cc(Cl)cc(C(F)(F)F)c2)CC1
1-(3-Chloro-5-trifluoromethyl-phenyl)-4-ethyl-piperazine

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Workup

  1. 1
    Otherthe title compound was recovered by the procedure

Procedure

Beginning with 1-(3-Chloro-5-trifluoromethyl-phenyl)-piperazine and iodoethane, the title compound was recovered by the procedure described in Example 2. MS m/z (rel. intensity, 70 eV)) 292 (M+, bp), 277 (88), 234 (33), 206 (55), 179 (49).

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: USRE041315E1uspto-grants-2010_05