Reaction #2200590

ord-7a3e402a4a8b4604936da49f3e7c46ea

Reaction equation

O=C(O)C(=O)Cc1cc2ccccc2[nH]1
indolepyruvic acid
CC(=O)C(=O)O
pyruvic acid
O=C(O)CC(=O)C(=O)O
oxalacetic acid
O=C(O)C(=O)CC(O)(Cc1c[nH]c2ccccc12)C(=O)O
4-(indol-3-ylmethyl)-4-hydroxy-2-oxoglutaric acid

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Procedure

According to the study by the present inventors, it has been found that PtALD can catalyze the aldol condensation reaction of indolepyruvic acid with pyruvic acid (or oxalacetic acid) to yield 4-(indol-3-ylmethyl)-4-hydroxy-2-oxoglutaric acid (IHOG), and the reaction of phenylpyruvic acid with pyruvic acid to yield 4-phenylmethyl-4-hydroxy-2-oxoglutaric acid (PHOG).

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07432100B2uspto-grants-2008_10