Reaction #2195482

ord-b755bca1dda84762a71ca2d1a13f56e7

Reaction equation

Cc1ccc(S(=O)c2ccc(C)cc2)cc1
bis(4-methylphenyl) sulfoxide
Cc1ccc(Cl)cc1
4-chlorotoluene
Cc1ccc([S+](c2ccc(C)cc2)c2ccc(C)cc2)cc1.[Cl-]
tris(4-methylphenyl)sulfonium chloride

Solvents

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Workup

  1. 1
    OtherThe target compound was obtained
  2. 2
    Otherthe procedure of Synthesis Example 1 aside
  3. 3
    Otherin Synthesis Example 1
  4. 4
    Extractionfor extraction

Procedure

The target compound was obtained by following the procedure of Synthesis Example 1 aside from using bis(4-methylphenyl) sulfoxide instead of the diphenyl sulfoxide and 4-chlorotoluene instead of the chlorobenzene in Synthesis Example 1, and increasing the amount of water for extraction.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07514202B2uspto-grants-2009_04