Reaction #215142

Reaction equation

lithium aluminum hydride

N-Cyclohexyl-N-nitrosoaniline

N-cyclohexylaniline

hydrazine

→

1-Cyclohexyl-1-phenyl-hydrazine

Conditions

Workup

1. 1
   workup.DISTILLATION1-Cyclohexyl-1-phenyl hydrazine distilled at 120°-150° C./0.2 mm

Procedure

N-Cyclohexyl-N-nitrosoaniline, prepared from N-cyclohexylaniline by the method described in Example 1 was subsequently reduced to the hydrazine by the lithium aluminum hydride method described in Example 4. 1-Cyclohexyl-1-phenyl hydrazine distilled at 120°-150° C./0.2 mm.

Source