Reaction #2139926

ord-30ba1818977d4670a24a24a0170e33ea

Reaction equation

C=COCC
Ethyl vinyl ether
OCc1ccccc1
benzyl alcohol
C=COCc1ccccc1
benzyl vinyl ether

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Workup

  1. 1
    ExtractionThe reaction mixture was extracted with ethyl acetate
  2. 2
    Extractionthe ethyl acetate extract
  3. 3
    Washwas washed with water
  4. 4
    workup.DISTILLATIONfollowed by distillation in vacuo

Procedure

Ethyl vinyl ether was mixed in benzyl alcohol, to which was then added mercury acetate, and the mixture was stirred at room temperature for 12 hours. The reaction mixture was extracted with ethyl acetate and the ethyl acetate extract was washed with water, followed by distillation in vacuo to obtain benzyl vinyl ether.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07326513B2uspto-grants-2008_02