Reaction #2139116

ord-287a84c34fb74da5b5d06cf202758e41

Reaction equation

C=CCCCC
1-hexene
C=CCCCCC
1-heptene
O=S(=O)(O)O
sulfuric acid
c1ccc2c(c1)Nc1ccccc1S2
phenothiazine
C=CC#N
acrylonitrile
→
C=CC(=O)NC(C)(CCCCC)C(C)CCCC
title product
C=CC(=O)NC(C)(CCCCC)C(C)CCCC
N-(α-methylpentyl,α-methyl-hexyl)acrylamide

Reactants

C=CCCCC
1-hexene
C=CCCCCC
1-heptene
O=S(=O)(O)O
sulfuric acid
c1ccc2c(c1)Nc1ccccc1S2
phenothiazine
C=CC#N
acrylonitrile

Reagents

None

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Procedure

Following a procedure analogous to that of Example 1, treat acrylonitrile with a mixture of 1-hexene and 1-heptene in the presence of 83% sulfuric acid and phenothiazine to obtain the title product.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04182790uspto-grants-1980_01