Reaction #1960492
ord-39843891419c41f6acc794de2578ff4d
Reaction equation
7,8-difluoro-2-pentyl-2H-chromene
→
7,8-difluoro-2-pentylchroman
Reactants
Reagents
Solvents
Conditions
Detailed conditions
See reaction.notes.procedure_details.
Workup
- 1OtherThe batch is evaporated to dryness
Procedure
51.0 g (0.21 mol) of 7,8-difluoro-2-pentyl-2H-chromene are hydrogenated at RT for 1 h in 510 ml of toluene in the presence of Pd/C (5% of Pd). The batch is evaporated to dryness: the crude product (yellowish liquid) can be used directly for the next step.