Reaction #1904078
ord-0754dff38c2f445d8aadbcb31972e151
Reaction equation
(2-amino-5-bromophenyl)(dithien-2-yl)methanol
bromoacetyl chloride
→
2-Bromo-N-{4-bromo-2-[hydroxy(dithien-2-yl)methyl]phenyl}acetamide
Reagents
None
Conditions
Detailed conditions
See reaction.notes.procedure_details.
Procedure
Prepared from (2-amino-5-bromophenyl)(dithien-2-yl)methanol and bromoacetyl chloride using the procedure described in example 1. 1H-NMR (DMSO-d6) δ 10.22 (s, 1H), 8.42 (s, 1H), 8.05 (d, J=9.0 Hz, 1H) 7.59 (m, 3H), 7.05 (m, 2H), 6.87 (m, 2H), 6.78 (d, J=3 Hz, 1H), 3.92 (s, 2H); MS (ES) m/z 484 (M−H)−.