Reaction #1904071
ord-5c3ba5a644b14ce595d16f6be7b8d35f
Reaction equation
1-(2-amino-5-bromo-phenyl)-ethanone
2-furyl lithium
→
1-(2-Amino-5-bromophenyl)-1-(2-furyl)ethanol
Reagents
None
Conditions
Detailed conditions
See reaction.notes.procedure_details.
Procedure
Prepared from 1-(2-amino-5-bromo-phenyl)-ethanone and 2-furyl lithium generally according to the procedure described in example 1. 1H-NMR (DMSO-d6) δ 7.6 (m, 1H), 7.08 (dd, J=2.73, 10.91 Hz, 1H), 6.8 (d, J=2.73 Hz, 1H), 6.56 (d, J=8.18 Hz, 1H), 6.45-6.38 (m, 2H), 6.14 (s, 1H), 5.3 (s, 2H), 1.76 (s, 3H); MS (ES) m/z 280/282 ([M−H]−, 30%).