Reaction #1880949

ord-e3da1ad9914a4f978033cb83e4daf5c9

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Workup

  1. 1
    OtherThe resultant reaction mixture
  2. 2
    Extractionwas extracted with ethyl acetate and water
  3. 3
    Washthe extract was washed with water
  4. 4
    workup.DISTILLATIONdistilled under reduced pressure

Procedure

Cyclohexylethyl alcohol was mixed with ethyl vinyl ether. Mercury acetate was added thereto and this mixture was stirred at room temperature for 12 hours. The resultant reaction mixture was extracted with ethyl acetate and water, and the extract was washed with water and then distilled under reduced pressure to obtain cyclohexylethyl vinyl ether (X-1) as the target compound.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07022456B2uspto-grants-2006_04