Reaction #1833278

ord-8de66611d8c64e55a13c4920a0f6d84a

Reaction equation

Cc1ccc(N(CCc2ccc(C)nc2)N=O)cc1
2-methyl-5-(N-nitroso-2-p-tolylaminoethyl)pyridine
O=S([O-])([O-])=S.[Na+].[Na+]
sodium thiosulfate
→
Cc1ccc(N(N)CCc2ccc(C)nc2)cc1
2-methyl-5-(N-amino-2-p-tolylaminoethyl)pyridine

Reactants

Cc1ccc(N(CCc2ccc(C)nc2)N=O)cc1
2-methyl-5-(N-nitroso-2-p-tolylaminoethyl)pyridine
O=S([O-])([O-])=S.[Na+].[Na+]
sodium thiosulfate

Reagents

None

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Procedure

reacting 2-methyl-5-(N-nitroso-2-p-tolylaminoethyl)pyridine with sodium thiosulfate to obtain 2-methyl-5-(N-amino-2-p-tolylaminoethyl)pyridine;

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US09149467B2uspto-grants-2015_10