Reaction #1810836
ord-1819011266ed44bbb0e0ad592c19e685
Reaction equation
3-ethoxy-4-methoxybenzaldehyde
acetic acid
4-amino-3-(2-fluorobenzylsulfanyl)-6-methyl-4H-1,2,4-triazin-5-one
→
4-[(3-ethoxy-4-methoxybenzylidene)amino]-3-(2-fluorobenzylsulfanyl)-6-methyl-4H-1,2,4-triazin-5-one
Reactants
Reagents
None
Solvents
Conditions
Temperature
65°CELSIUS
Detailed conditions
See reaction.notes.procedure_details.
Workup
- 1FiltrationThe resultant precipitate was filtered off with suction
Procedure
0.054 g of 3-ethoxy-4-methoxybenzaldehyde and 0.017 ml of acetic acid were added to a solution of 0.080 g of 4-amino-3-(2-fluorobenzylsulfanyl)-6-methyl-4H-1,2,4-triazin-5-one in 4 ml of ethanol, and the mixture was stirred at 65° C. The resultant precipitate was filtered off with suction, giving 4-[(3-ethoxy-4-methoxybenzylidene)amino]-3-(2-fluorobenzylsulfanyl)-6-methyl-4H-1,2,4-triazin-5-one.