Reaction #1726660

ord-7d7570892ebf418f905cbd5615a71312

Reaction equation

CC(=O)O.CC(=O)O.[Pd]
palladium(II) acetate trimer
CCC(=O)O
propionic acid
→
CCC(=O)[O-].CCC(=O)[O-].[Pd+2]
Palladium(II) Propionate

Reactants

CC(=O)O.CC(=O)O.[Pd]
palladium(II) acetate trimer
CCC(=O)O
propionic acid

Reagents

None

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Workup

  1. 1
    TemperatureThe mixture was maintained at 40 degrees Celsius for 24 hours
  2. 2
    OtherExcess propionic acid was removed under vacuum at room temperature

Procedure

5 gm commercial palladium(II) acetate trimer (Aldrich) was added to 40 g of propionic acid. The mixture was maintained at 40 degrees Celsius for 24 hours. Excess propionic acid was removed under vacuum at room temperature. The resulting yellow solid was used for making palladium inks.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08110254B1uspto-grants-2012_02