Reaction #166019

ord-97e83a8c3a8e47f1a98c2fc1460c4b20

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Workup

  1. 1
    OtherLC/MS [8.75 min; 404 (M+1)]

Procedure

N-methoxy-3-(2-chloro-4-iodo-phenylamino)-isonicotinamide was synthesized according to the procedure for General Method 1, outlined above, starting with 0.30 mmol of 3-[(2-chloro-4-iodophenyl)amino]isonicotinic acid (intermediate 2) and 0.42 mmol of O-methyl-hydroxylamine. LC/MS [8.75 min; 404 (M+1)]

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08841459B2uspto-grants-2014_09