Reaction #166017

ord-cae86a4ae910477c8df1a6b5f3953d9c

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Workup

  1. 1
    OtherLC/MS [9.30 min; 430 (M+1)]

Procedure

N-allyloxy-3-(2-chloro-4-iodo-phenylamino)-isonicotinamide was synthesized according to the procedure for General Method 1, outlined above, starting with 0.20 mmol of 3-[(2-chloro-4-iodophenyl)amino]isonicotinic acid (intermediate 2) and 0.36 mmol of O-allyl-hydroxylamine. LC/MS [9.30 min; 430 (M+1)]

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08841459B2uspto-grants-2014_09