Reaction #164422

ord-7a956f8afc4047d8a9f5176f69542df7

Reaction equation

CC(=O)[O-].CC(=O)[O-].[Ni+2]
nickel acetate
CCCCCCCC/C=C\CCCCCCCC(=O)O
oleic acid
→
CCCCCCCC/C=C\CCCCCCCC(=O)[O-].CCCCCCCC/C=C\CCCCCCCC(=O)[O-].[Ni+2]
nickel (II) oleate

Reactants

CC(=O)[O-].CC(=O)[O-].[Ni+2]
nickel acetate
CCCCCCCC/C=C\CCCCCCCC(=O)O
oleic acid

Reagents

None

Conditions

Temperature
150°CELSIUS
Detailed conditions
See reaction.notes.procedure_details.

Workup

  1. 1
    OtherNickel (II) oleate is prepared
  2. 2
    Otherto evaporate the acetic acid

Procedure

Nickel (II) oleate is prepared by mixing 2.48 g of nickel acetate and 5.64 g of oleic acid with stirring for about one hour. The mixture is heated to about 150° C. to evaporate the acetic acid and form a transparent liquid of nickel (II) oleate. Nickel (II) oleate can also be prepared by mixing 2.57 g of nickel acetylacetonate and 5.64 g of oleic acid with stirring. The mixture is then heated to evaporate the acetylacetonate and form a transparent liquid of nickel (II) oleate.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08840816B2uspto-grants-2014_09