Reaction #1597018

ord-9ad6a617d9cf491f86cecb0d7b628fe5

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Workup

  1. 1
    OtherThis material was prepared

Procedure

This material was prepared according to the method of Example 1 using 5-chlorosalicylic acid and 3-ethylaniline, with reagents and solvents employed in similar molar ratios. 1HNMR (500 MHz, DMSO-d6): δ 1.20 (t, 3H), 2.62 (q, 1H), 7.02 (m, 2H), 7.28 (m, 1H), 7.47 (m, 1H), 7.54 (m, 1H), 7.56 (br s, 1H), 7.90 (m, 1H), 10.34 (s, 1H).

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08211882B2uspto-grants-2012_07