Reaction #1597016

ord-46521701bd6a429db9f8176d19f5783f

Reaction equation

O=C(O)c1cc(Cl)cc(Cl)c1O
3,5-dichlorosalicylic acid
Nc1ccc([N+](=O)[O-])cc1Cl
2-chloro-4-nitroaniline
→
O=C(Nc1ccc([N+](=O)[O-])cc1Cl)c1cc(Cl)cc(Cl)c1O
3,5-dichloro-N-(2-chloro-4-nitrophenyl)-2 hydroxybenzamide

Reactants

O=C(O)c1cc(Cl)cc(Cl)c1O
3,5-dichlorosalicylic acid
Nc1ccc([N+](=O)[O-])cc1Cl
2-chloro-4-nitroaniline

Reagents

None

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Workup

  1. 1
    OtherThis material was prepared

Procedure

This material was prepared according to the method of Example 1 using 3,5-dichlorosalicylic acid and 2-chloro-4-nitroaniline, with reagents and solvents employed in similar molar ratios. 1HNMR (500 MHz, DMSO-d6): δ7.85 (m, 1H, H4), 7.98 (m, 1H, H5), 8.29 (m, 1H, H5′), 8.04 (m, 1H, H6), 8.44 (m, 1H, H3′), 8.55 (m, 1H, H6′).

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08211882B2uspto-grants-2012_07