Reaction #155688

ord-abf097ba25764dcba35fabf3012c92c3

Reaction equation

Brc1ccc(-c2ccc3c(ccc4ccccc43)c2)cc1
2-(4-bromophenyl)phenanthrene
OB(O)c1cccc2c1ccc1ccccc12
phenanthrene-1-boronic acid
→
Brc1ccc(-c2cccc3c2ccc2ccccc23)cc1
1-(4-bromophenyl)phenanthrene

Reactants

Brc1ccc(-c2ccc3c(ccc4ccccc43)c2)cc1
2-(4-bromophenyl)phenanthrene
OB(O)c1cccc2c1ccc1ccccc12
phenanthrene-1-boronic acid

Reagents

None

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Workup

  1. 1
    OtherSynthesis

Procedure

Synthesis was performed in the same manner as in the synthesis of 2-(4-bromophenyl)phenanthrene except that phenanthrene-1-boronic acid was used instead of phenanthrene-2-boronic acid.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08822041B2uspto-grants-2014_09