Reaction #155687

ord-7994827070c341bcba9d8d3d38a24134

Reaction equation

OB(O)c1ccc2c(ccc3ccccc32)c1
phenanthrene-2-boronic acid
Brc1cccc2c1ccc1ccccc12
1-bromophenanthrene
→
OB(O)c1cccc2c1ccc1ccccc12
phenanthrene-1-boronic acid

Reactants

OB(O)c1ccc2c(ccc3ccccc32)c1
phenanthrene-2-boronic acid
Brc1cccc2c1ccc1ccccc12
1-bromophenanthrene

Reagents

None

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Workup

  1. 1
    OtherSynthesis

Procedure

Synthesis was performed in the same manner as in the synthesis of phenanthrene-2-boronic acid except that 1-bromophenanthrene was used instead of 2-iodophenanthrene.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08822041B2uspto-grants-2014_09