Reaction #155394

Reaction equation

3-tert-butyldimethylsilyloxybenzoic acid

thionyl chloride

→

3-tert-Butyldimethylsilyloxybenzoyl chloride

Conditions

Workup

1. 1
   Temperaturewas heated
2. 2
   Temperatureat reflux for 1 hr 30 min
3. 3
   ConcentrationThe reaction mixture was concentrated under reduced pressure
4. 4
   Otherto yield 5.77 parts of an oil

Procedure

Into a 100 mL round bottom flask a mixture of 5 parts of 3-tert-butyldimethylsilyloxybenzoic acid and 25 mL of thionyl chloride was heated at reflux for 1 hr 30 min. The reaction mixture was concentrated under reduced pressure to yield 5.77 parts of an oil.

Source