Reaction #155389

ord-caa76cac44bd4535bba3bcf39fa8fc54

Reaction equation

COC(=O)C1c2ccccc2N(C)c2ccccc21
4-phenylphenol
COC(=O)C1c2ccccc2N(C)c2ccccc21
methyl 10-methylacridan-9-carboxylate
CN1c2ccccc2C(C(=O)O)c2ccccc21.c1ccc(-c2ccccc2)cc1
4,4′-biphenyl 10-methylacridan-9-carboxylate

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Procedure

A solution of 0.24 parts of 10-methylacridan-9-carboxylic acid chloride(78) in 10 mL dichloromethane and 0.145 parts of 4-phenylphenol (76) in 5 mL of dichloromethane and 1 mL of tetrahydrofuran is treated as described in example I, to give 0.21 parts of 4,4′-biphenyl 10-methylacridan-9-carboxylate. This compound has the following structure.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08822233B2uspto-grants-2014_09