Reaction #1509645

ord-f6f3807a53504064978aa6558408ba26

Reaction equation

CCCCBr
1-bromobutane
c1ccncc1
pyridine
→
CCCC[n+]1ccccc1.[Br-]
Butylpyridinium bromide

Reactants

CCCCBr
1-bromobutane
c1ccncc1
pyridine

Reagents

None

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Workup

  1. 1
    OtherThe solid obtained
  2. 2
    Otheris dried under low vacuum at 50° C.

Procedure

Butylpyridinium bromide is prepared by a Menshutkin reaction of 27.5 g of 1-bromobutane with 15.8 g of pyridine at 40° C. in 24 hours, without solvent. The solid obtained is dried under low vacuum at 50° C.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08927160B2uspto-grants-2015_01