Reaction #1379901

ord-f7b914a1905a4d9e9f10b720b5dd5864

Reaction equation

CCCCCCCCCCC1CC2C=CC1C2
5-decyl-2-norbornene
CC=C1CC2C=CC1C2
5-ethylidene-2-norbornene
CCCCCCC1CC2C=CC1C2
5-hexyl-2-norbornene
CC=C1CC2C=CC1C2.CCCCCCC1CC2C=CC1C2
HNB ENB
C1=CC2CCC1C2
norbornene

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Workup

  1. 1
    OtherPolymerization
  2. 2
    workup.ADDITIONwere added

Procedure

Polymerization was conducted in the same manner as in Preparation Example 1 except that 18 parts of 5-hexyl-2-norbornene (HNB) was used in place of 26 parts of 5-decyl-2-norbornene, and 3 parts of 5-ethylidene-2-norbornene (ENB) were added, thereby obtaining 21 parts of a norbornene terpolymer [Mn=71,100, Mw=107,000; compositional ratio NB/HNB/ENB of monomers=74/23/3 (molar ratio); Tg=323° C.] was obtained.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07238405B2uspto-grants-2007_07