Reaction #1365706

ord-8df9a23df07745eab43ba41bd6dfb9e9

Reaction equation

COc1ccc(C=O)cc1
Anisaldehyde
CC(=O)O
acetic acid
O=S(=O)(O)O
sulfuric acid
→
COc1ccc(C=O)cc1.O=S(=O)(O)O
Anisaldehyde sulfuric acid

Reactants

COc1ccc(C=O)cc1
Anisaldehyde
CC(=O)O
acetic acid
O=S(=O)(O)O
sulfuric acid

Reagents

None

Solvents

CO
methanol

Conditions

Temperature
100°CELSIUS
Detailed conditions
See reaction.notes.procedure_details.

Procedure

Anisaldehyde (0.5 ml) is mixed with glacial acetic acid (10 ml), methanol (85 ml) and concentrated sulfuric acid (5 ml). This solution is sprayed onto the TLC plate, which is then heated at 100° C.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06444233B1uspto-grants-2002_09