Reaction #1265370

ord-185bd575ca1b4685a41e83657f54ad98

Reaction equation

O=Cc1cccc(C(=O)O)c1
3-formyl benzoic acid
CCCNCCC
di-n-propylamine
→
CCCN(CCC)C(=O)c1cccc(C=O)c1
title compound
CCCN(CCC)C(=O)c1cccc(C=O)c1
N,N-di-n-propyl-3-formylbenzamide

Reactants

O=Cc1cccc(C(=O)O)c1
3-formyl benzoic acid
CCCNCCC
di-n-propylamine

Reagents

None

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Procedure

To 2 g (13.3 mmole) of 3-formyl benzoic acid was coupled with di-n-propylamine via Method I to give 2.5 g of the title compound as a white solid.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07276484B2uspto-grants-2007_10