Reaction #1265364

ord-2c223fefb7074d8eb34fda418bec8dd5

Reaction equation

OCCN1CCOCC1
2-morpholinoethanol
O=C(Cl)c1ccc(-c2ccccc2)cc1
4-phenylbenzoyl chloride
O=C(OCCN1CCOCC1)c1ccc(-c2ccccc2)cc1
2-morpholinoethyl 4-phenylbenzoate
Yield 93.0%

Conditions

Detailed conditions
See reaction.notes.procedure_details.

Workup

  1. 1
    OtherThe procedure of Synthesis Example 1

Procedure

The procedure of Synthesis Example 1 was repeated except that 2-morpholinoethanol was used instead of the triethanolamine, and 4-phenylbenzoyl chloride was used instead of the benzoyl chloride, to give 2-morpholinoethyl 4-phenylbenzoate in a yield of 93%.

Source

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07276324B2uspto-grants-2007_10